PESTICIDE RESIDUES IN FOOD - 1982 Sponsored jointly by FAO and WHO EVALUATIONS 1982 Data and recommendations of the joint meeting of the FAO Panel of Experts on Pesticide Residues in Food and the Environment and the WHO Expert Group on Pesticide Residues Rome, 23 November - 2 December 1982 Food and Agriculture Organization of the United Nations Rome 1983 ANNEX I ACCEPTABLE DAILY INTAKES, MAXIMUM RESIDUE LIMITS AND GUIDELINE LEVELS PROPOSED AT THE 1982 MEETING These figures are additional to, or amend, those recorded in Annexes of the reports of earlier meetings. Limits recommended at meetings from 1965-1977 inclusive are summarized in document FAO/WHO 1978c. This table includes maximum acceptable daily intake (ADIs), maximum residue limits (MRLs) and guideline levels (GLs). These terms are defined in Annex III of the Report of the 1975 Meeting. Part 1 lists ADIs and MRLs. Some ADIs and MRLs are temporary; in these cases the year in which further data are required is specified in parenthesis below the ADI. Part 2 lists GLs. New, as distinct from amended, recommendations are identified by the symbol * before the commodity or before the ADI. Residue levels at or about the limit of determination are followed by the symbol **. Amended recommendations are followed by the previous recommendation in parenthesis. PART 1. ACCEPTABLE DAILY INTAKES(ADIs) and MAXIMUM RESIDUE LIMITS (MRLs) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) acephate 0.003 ADI replaced by temporary 1976, 1979 (1984) ADI at lower level. 1981 MRLs replaced by temporary MRLs. aldicarb 0.005 *maize 0.05 ADI increased. MRLs are 1979 *pecans 0.5 for the sum of aldicarb, its *sorghum 0.2 sulphoxide and its sulphone, *sweet potatoes 0.1 determined as aldicarb sulphone and expressed as *maize fodder 2 on a dry aldicarb. *maize forage 20 weight *sorghum fodder 0.5 basis azocyclotin 0.003 apples 2 (0.1**) MRLs (including those 1979, 1981 beans 0.5(0.2 for previously recommended) are for the sum of kidney beans) azocyclotin, cyhexatin strawberries 2 (0.1**) and dicyclohexyltin oxide expressed as cyhexatin. (Note the amended residue definition.) PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) bendiocarb *0.002 *barley 0.05** Temporary MRLs are for *maize 0.05** unconjugated bendiocarb in *mushrooms 0.1 commodities of plant *oats 0.05** origin, and for the sum of *pome fruit 0.02** conjugated and unconjugated *potatoes 0.05** bendiocarb, 2,2-dimethyl- *rice (in husk) 2 1,3-benzoxodiol-4-ol and *sugar beets 0.05** N-hydroxymethyl-bendiocarb *wheat 0.05** expressed as bendiocarb, in commodities of animal *barley straw 0.05** origin. All MRLs, except *maize fodder those for maize, sugar and forage 0.05** beets, maize fodder and *oat straw 0.05** sugar beet tops are *rice straw 1 temporary until the *sugar beet leaves 0.05** required information on *wheat straw 0.05** nationally approved agricultural practices *cattle, carcase (see "Further work or meat 0.05** information") is provided, *cattle, fat 0.05** irrespective of the status *cattle, kidney 0.2** of the ADI. *cattle, meat Limit for mushrooms byproducts reflects maximum residues (except kidney) 0.05** expected from wall PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) bendiocarb *eggs 0.05** treatment prior to (con't) *milk 0.05** establishment of crop. *poultry, meat 0.05** *poultry, fat 0.05** *poultry byproducts 0.05** binapacryl No ADI ADI withdrawn. MRLs 1969, 1974 replaced by GLs. See Part 2 of Annex. bromophos 0.04 apples 5 (2) MRLs are for bromophos. 1972, 1975, carrots 2 (1) Metabolites are not 1977 cereal grains 10 included. cherries 1 (0.5) The commodity description *kale 0.5 "cereal grains" lettuce 2 (0.5) replaces "raw grain". onions 0.5 (0.1) The MRL is unchanged. peaches 1 (0.5) plums 5 (1) *raspberries 1 spinach 2 (1) *tomatoes 0.5 *barley straw 0.5 *oat straw 0.5 *pea fodder 0.5 *sugar beet leaves 0.5 milk 0.05** (0.02**) PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) captafol 0.01 ADI replaced by 1969, 1973, (1985) temporary ADI at lower 1974, 1976, level. MRLs replaced 1977 by temporary MRLs. captan 0.01 ADI replaced by 1965, 1969, (1984) temporary ADI at lower 1973, 1974, level. MRLs replaced 1977, 1978, by temporary MRLs. 1980 carbofuran 0.01 ADI maintained at same 1976, 1979, level. 1980 chlordane 0.001 ADI replaced by 1965, 1967, (1984) temporary ADI at same 1969, 1970, level. MRLs replaced 1972, 1974, by temporary MRLs. 1977 chlorpyrifos 0.01 milk 0.01** ADI increased. 1972, 1974, (previously The MRL is for 1975, 1977, 0.1 on a chlorpyrifos. Metabolites 1981 fat basis) are not included. PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) cyhexatin 0.008 MRLs for cyhexatin are 1970, 1973, now for the sum of 1974, 1975, 1977, cyhexatin and dicyclohexyltin 1978, 1980, oxide, expressed 1981 as cyhexatin. Note the amended residue definition. cypermethrin 0.05 *barley 0.5 MRLs are for cypermethrin 1979, 1981 *currants (black, (sum of isomers). red and white) 0.5 Metabolites *gooseberries 0.5 are not included. The *kidney beans group MRL for root and (in pod) 0.5 tuber vegetables *leeks 0.5 replaces previous *mushrooms 0.05 limits for potatoes *oilseeds 0.2 and sugar beet. That *onions 0.1 for oilseeds replaces *peanuts 0.02 MRLs for cottonseed *root and tuber and rapeseed at the same vegetables 0.05 level and the group limit *spinach 2 for edible vegetable oils replaces the limit for *eggs 0.05 cottonseed oil (edible). *poultry meat 0.05 *edible vegetable oils 0.5 PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) deltamethrin *0.01 *artichokes 0.05 An ADI has now been 1980, 1981 *assorted fruits - estimated thus previously edible peel 0.1 recorded GLs are replaced *bananas 0.05 by MRLs. These are for *brassica leafy deltamethrin. Metabolites vegetables 0.05 are not included. *bulb vegetables 0.1 *cereal grains 2 *clementines 0.05 *cocoa beans 0.05 *coffee beans 2 *fruiting vegetables - edible peel 0.05 *grapes 0.05 *hops (dry) 5 *kiwi fruit 0.05 *leafy vegetables 0.2 *legume oilseeds 0.01 *legume vegetables 0.1 *melons 0.01 *mushrooms 0.01 *oilseeds 0.1 *oranges, sweet 0.05 *pineapples 0.01 *pome fruits 0.1 *root and tuber vegetables 0.01 PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) deltamethrin *stone fruits 0.05 1980,1981 *strawberries 0.05 *tea 10 *cereal straw 0.5 *legume animal 0.5 (dry feeds (weight basis) *wheat bran 5 *wheat flour (white) 0.5 *wheat flour (wholemeal) 2 demeton and No ADI ADIs for demeton and related compounds for the sum of demeton- (demeton, S-methyl, oxydemeton- demeton-S-methyl, methyl and demeton-S- oxydemeton-methyl methyl sulphone withdrawn. and demeton-S- Corresponding MRLs methyl sulphone) replaced by GLs. See part 2 of Annex. PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) demeton: 1965, 1967,1975 demeton-S-methyl: 1973, 1979 oxydemeton- methyl: 1965 (as demeton-S-methyl sulphoxide), 1967, 1968, 1973 demeton-S-methyl sulphone: 1973 dialifos No ADI ADI withdrawn. MRLs 1976 replaced by GLs. See part 2 of Annex. dichlofluanid 0.3 Temporary ADI extended at 1969, 1974, (1983) same level. Previously 1977, 1979, required residues data 1981 have been supplied. All MRLs remain temporary until an ADI is estimated. diphenylamine 0.02 ADI replaced by temporary 1969, 1976, (1984) ADI at same level. MRLs 1979 replaced by temporary MRLs. PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) endosulfan 0.008 ADI replaced by temporary 1965, 1967, (1985) ADI at same level. It is 1968, 1971, for the sum of alpha- 1974, 1975 endosulfan, beta-endosulfan and endosulfan sulphate. MRLs replaced by temporary MRLs. ethiofencarb 0.1 brassicas (except Temporary ADI replaced by 1977, 1978, Chinese cabbage) 2 (5) ADI at same level. 1981 Chinese cabbage 5 Temporary MRLs replaced by MRLs. ethion 0.001 ADI replaced by temporary 1968, 1969, (1985) ADI at lower level. MRLs 1970, 1972, replaced by temporary MRLs. 1975 etrimfos 0.003 *apples 0.5 Temporary ADI replaced *apricots 0.2 by ADI at same level. *artichokes 0.5 Previous temporary MRLs *beans 0.2 replaced by MRLs. All *Brussels sprouts 0.5 MRLs are for the sum of *cabbage 0.1 etrimfos, its oxygen *cabbage, Chinese 0.1 analogue and 6-ethoxy-2- *cauliflower 0.2 ethyl-4-hydroxypyrimidine, *cherries 0.01** expressed as etrimfos. *cucumbers 0.1 Attention is drawn to PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) etrimfos *grapes 0.5 the amended residue (con't) *kale 0.1 definition. *kohlrabi 0.01** *leeks 0.1 *lettuce 0.5 *onions 0.1 *peaches 0.1 *peas 0.2 *plums 0.2 *potatoes 0.1 *radishes 0.1 *rice 0.1 *soybeans 0.01** *sugar beets 0.01** *tomatoes 0.2 *sugar beet leaves 0.01** *eggs 0.01** *poultry meats 0.02** fenitrothion 0.001 ADI replaced by 1969, 1974, (1984) temporary ADI at lower 1976, 1977, level. MRLs replaced 1979 by temporary MRLs. fensulfothion 0.0003 ADI maintained at same 1972 level. PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) fenvalerate 0.007 Temporary ADI extended 1979, 1981 (1985) at same level. folpet 0.1 ADI replaced by 1969, 1973, (1984) temporary ADI at 1974 same level. MRLs replaced by temporary MRLs. isofenphos 0.0005 *citrus fruit 1 Temporary ADI extended 1981 (1986) *pears 0.5 at same level. *bananas 0.02** Temporary MRLs are for the sum of isofenphos and its oxygen analogue. metalaxyl *0.03 *avocados 0.1** MRLs are for metalaxyl. *broccoli 0.5 Metabolites are not *cabbage 0.5 included. *cauliflower 0.5 *cereal grains 0.05** *citrus fruits 5 *cucumbers 0.5 *gherkins 0.5 *grapes 5 *hops (dried) 10 *lettuce 2 *melon 0.2 PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) metalaxyl *onions 0.05 (con't) *peas 0.05** *potatoes 0.1 *spinach 1 *squash 0.2 *sugar beets 0.05** *sunflower seed 0.05** *tomatoes 0.5 *watermelons 0.2 methacrifos 0.0003 Temporary ADI extended (1986) at same level. methamidophos 0.0004 ADI replaced by temporary 1976, 1979, (1985) ADI at lower level. MRLs 1981 replaced by temporary MRLs. paraquat 0.001 ADI replaced by temporary 1970, 1972, (1985) ADI at lower level. 1976, 1978, Temporary ADI is for 1981 paraquat dichloride. It is equivalent to 0.0007 mg/kg bw for paraquat ion. MRLs replaced by temporary MRLs. PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) parathion-methyl 0.001 Temporary ADI extended at 1965, 1968, (1984) same level. 1972, 1975, 1979, 1980 permethrin 0.05 *almonds 0.1 Temporary ADI replaced by 1979, 1980, The ADI *asparagus 1 ADI at higher level. 1981 applies grapes 2 (1) Temporary MRLs replaced by only to *horseradish 0.5 MRLs. They are for the leeks 0.5 (5) permethrin (sum of nominal lettuce 10 (20) isomers). Metabolites 40% cis-, *olives 1 are not included. 60% trans- *sunflower seed 1 The requirement for adequate material *sunflower seed data on use patterns oil (crude (1979) has now been met. and refined) 1 phorate *0.0002 *barley 0.05 As a temporary ADI has 1977 (1983) *beans 0.1 been estimated, previously *carrots 0.5 recorded GLs are *celery 0.1 replaced by temporary *cottonseed 0.05 MRLs. *cowpea 0.1 *egg plants 0.1 *grapes 0.05 *hops, dried 0.1 *lettuce 0.2 PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) phorate *maize (green) 0.05 1977 *peanuts 0.05 (con't) *potatoes 0.05 *rapeseed 0.1 *sorghum 0.05 *soybeans 0.05 *sugar beets 0.05 *tomatoes 0.1 *wheat 0.05 *alfalfa (dry) 1 *fodder beet 0.05 *sugar beet leaves 1 *eggs 0.05** *meat 0.05** *milk 0.05** phosphamidon 0.001 ADI replaced by 1965, 1966, (1985) temporary ADI at same 1968, 1969, level. MRLs replaced 1972, 1974 by temporary MRLs. phoxim *0.0005 No MRLs estimated. (1984) PART 1. (con't) Pesticide and ADI Commodity Recommended Remarks date of (mg/kg MRL previous body (mg/kg) evaluations weight) pirimicarb 0.02 Temporary ADI replaced 1976, 1978, by ADI at higher level. 1979, 1981 Temporary MRLs replaced by MRLs. propargite 0.15 tea (dried) 10 (5) Temporary ADI replaced 1977, 1978, by ADI at higher level. 1979, 1980 Temporary MRLs replaced by MRLs. These are for propargite. Metabolites are not included. triazophos *0.0002 No MRLs estimated. (1986) vamidothion *0.0003 *apples 2 As a temporary ADI has 1973 (1985) *Brussels sprouts 1 estimated previously *grapes 0.5 recorded GLs are replaced *pears 2 by temporary MRLs. *sugar beets 0.5 PART 2. - GUIDELINE LEVELS (GLs) NO ADIs Pesticide and Commodity Remarks date of GL previous (mg/kg) evaluations binapacryl apples 0.5 As the ADI for binapacryl 1969, 1974 cherries 0.5 has been withdrawn by the grapes 0.5 1982 JMPR, the previously nectarines 0.3 recommended MRLs are peaches 1 replaced by GLs. pears 0.5 plums 0.3 demeton apples 0.5 As the ADI for demeton 1965, 1967, apricots 1 has been withdrawn by the 1975 citrus fruit 0.5 1982 JMPR, the previously grapes 1 recommended MRLs are melons 0.1 replaced by GLs. peaches 1 pears 0.5 plums 0.2 strawberries 0.1 demeton-S-methyl apples 1 As the ADI for these compounds 1973, 1979 beans 0.2 has been withdrawn oxydemeton-methyl blackberries 0.5 by the 1982 JMPR, the previously 1965, 1967, broccoli 0.2 recommended MRLs 1968, 1973 and Brussels sprouts 0.2 are replaced by GLs. demeton-S-methyl cabbage 0.2 sulphone cantaloupes 0.2 1973 cauliflower 0.2 citrus fruit 0.5 cottonseed 0.1 PART 2. (con't) Pesticide and Commodity Remarks date of GL previous (mg/kg) evaluations demeton-S-methyl cucumbers 0.2 1973, 1979 currants (black, oxydemeton-methyl red and white) 2 1965, 1967, egg plants 0.2 1968, 1973 and gooseberries 0.5 demeton-S-methyl grapes 2 sulphone lettuce 0.5 1973 nuts (shelled) 0.05** (con't) peaches 1 pears 0.5 peas 0.2 plums 1 potatoes 0.2 pumpkin 0.2 raspberries 0.5 raw cereals 0.2 strawberries 0.5 sugar beets 0.1 summer squash 0.5 turnips 0.1 watermelons 0.2 winter squash 0.2 alfalfa fodder 5 clover fodder 5 maize fodder and straw 5 sorghum fodder 5 PART 2. (con't) Pesticide and Commodity Remarks date of GL previous (mg/kg) evaluations demeton-S-methyl sugar beet leaves 5 1973, 1979 turnip leaves oxydemeton-methyl (used as animal 1965, 1967, feed) 5 1968, 1973 and carcase meat: demeton-S-methyl cattle, pigs, sulphone sheep 0.05** 1973 fat of cattle, (con't) pigs, sheep 0.05** poultry meat 0.05** poultry fat 0.05** eggs 0.05** milk 0.05** milk products 0.05** dialifos apples 2 As the ADI for dialifos 1976 citrus fruit 3 has been withdrawn by the grapes 1 1982 JMPR, the previously pears 2 recommended MRLs are pecans 0.01** replaced by GLs. raisins 2 apple pomace (dried) 40 citrus pulp (dried) 15 grape pomace (dried) 20 PART 2. (con't) Pesticide and Commodity Remarks date of GL previous (mg/kg) evaluations dialifos cattle, fat 0.2 1976 eggs 0.01** (con't) milk 0.01 poultry, fat 0.05** poultry, meat 0.05** sheep, fat 0.2 ANNEX II PREVIOUS FAO AND WHO DOCUMENTATION FAO/WHO - Procedures for the testing of intentional food additives to 1958 establish their safety for use. Second report of the Joint FAO/WHO Expert Committee on Food Additives. FAO Nutrition Meetings Report Series, No. 17: WHO Technical Report Series, No. 144. FAO/WHO - Evaluation of the carcinogenic hazards of food additives. 1961 Fifth Report of the Joint FAO/WHO Expert Committee on Food Additives. FAO Nutrition Meetings Report Series, No. 29: WHO Technical Report Series, No. 220. FAO/WHO - Principles governing consumer safety in relation to 1962 pesticide residues. Report of a meeting of a WHO Expert Committee on Pesticide Residues held jointly with the FAO Panel of Experts on the Use of Pesticides in Agriculture. FAO Plant Production and Protection Division Report, No. PL:1961/11: WHO Technical Report Series,No.240. FAO/WHO - Evaluation of the toxicity of pesticide residues in food; 1964 report of a Joint Meeting of the FAO Committee on Pesticides in Agriculture and the WHO Expert Committee on Pesticide Residues. FAO Meeting Report, No. PL:1963/13: WHO Food Add./23 (1964). FAO/WHO - Evaluation of the toxicity of pesticide residues in food. 1965a Report of the Second Joint Meeting of the FAO Committee on Pesticides in Agriculture and the WHO Expert Committee on Pesticide Residues. FAO Meeting Report, No. PL:1965/10: WHO Food Add./26.65. FAO/WHO - Evaluations of the toxicity of pesticide residues in food. 1965b FAO Meeting Report, No. PL:1965/10/1: WHO Food Add./27.65. FAO/WHO - Evaluation of the hazards to consumers resulting from the 1965c use of fumigants in the protection of food. FAO Meeting Report, No. PL:1965/10/2: WHO Food Add./28.65. FAO/WHO - Pesticide residues in food. 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Report of the 1979 Joint Meeting 1980a of the FAO Panel of Experts on Pesticide Residues in Food and the Environment and the WHO Expert Group on Pesticide Residues. FAO Plant Production and Protection Paper 20. FAO/WHO - 1979 evaluations of some pesticide residues in food. FAO 1980b Plant Production and Protection Paper 20 Sup. FAO/WHO - Pesticide residues in food. Report of the 1980 Joint Meeting 1981a of the FAO Panel of Experts on Pesticide Residues in Food and the Environment and the WHO Expert Group on Pesticide Residues. FAO Plant Production and Protection Paper 26. FAO/WHO - 1980 evaluations of some pesticide residues in food. FAO 1981b Plant Production and Protection Paper 20 Sup. FAO/WHO - Pesticide residues in food. Report of the 1981 Joint Meeting 1982a of the FAO Panel of Experts on Pesticide Residues in Food and the Environment and the WHO Expert Group on Pesticide Residues. FAO Plant Production and Protection Paper 37. 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See Also: Toxicological Abbreviations